Isolation and structural characterization of the endohedral fullerene Sc3N@C78
AuthorOlmstead, Marilyn M.; de Bettencourt-Dias, Ana; Duchamp, James C.; Stevenson, Steven; Marciu, Daniela; Dorn, Harry C.; Balch, Alan L.
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The endohedral fullerene Sc3N@C78 was prepd., isolated and characterized by its 13C NMR, UV/Vis and mass spectra. Black crystals of Sc3N@C78.cntdot.[Co(oep)].cntdot.1.5C6H6.cntdot.0.3CHCl3 were obtained (H2oep = octaethylporphyrin) and the crystal structure was detd. showing that the C78 is the D3h (78:5) isomer.